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Food Safety Tech

Call for Abstracts: Be a Part of the 2019 Food Safety Supply Chain Conference

By Food Safety Tech Staff
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Food Safety Tech

The supply chain is a potentially weak and vulnerable part of a company’s food safety plan. The annual Food Safety Supply Chain Conference is months away and we are accepting abstracts for presentations. The conference takes place May 29–30, 2019 in Rockville, MD.

If you have expertise in the following areas, we invite you to submit an abstract to present at the conference:

  • Food Safety Supply Chain Vulnerabilities & Solutions
  • Audits & Inspections
  • How to Write Supplier Specifications
  • Blockchain Technology
  • FSMA’s Sanitary Transportation Compliance Tools & Techniques
  • Supply Chain Traceability
  • FSMA’s FSVP Compliance Tools & Best Practices
  • Data, Predictive Analysis
  • Recalls: barcode labeling, case histories and lessons learned
  • Testing Strategies of the Supply Chain
  • Supplier Verification Best Practices
  • Supply Chain Risk Management
  • Food Safety Transportation, Distribution and Logistics
  • Food Authenticity
  • Food Safety/Quality Culture measurement in supplier management
  • Supplier Management Case Histories

Each abstract will be judged based on educational merit. The submission deadline is February 8, 2019.

Shawna Wagner, DNV GL
FST Soapbox

Did You Write “NONE” for Biological, Chemical and Physical Hazards in Your HACCP Plan?

By Shawna Wagner
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Shawna Wagner, DNV GL

Ok, ok I know what you are thinking, another article about HACCP. You have been HACCP certified since 1999 and doing this for years—why read this article? That golden sticker on your certificate does not last forever. Industry has changed, approaches to food safety have changed, and your HACCP plan should have evolved. Did it?

Biological, chemical, physical, biological, chemical, and physical hazards. If you are any part of the quality assurance or HACCP team, you can recite this in your sleep. Do you recite economical and radiological hazards? These are one of the most commonly missed items in a plant’s HACCP plan that I have witnessed when auditing. This, of course, applies only to plants that must comply with FSMA, but does it truly hurt to think about including it in all plants? I mean, we are all in this for food safety, right?!

In speaking about radiological hazards, most of the time I will have site management tell me that I am not by a power plant so there are not hazards to my operations. If you are a producer of vegetables and fruits, or a plant receiving these kinds of ingredients, water and even soil can be a home to radioactive hazards! Radioactive minerals are naturally occurring and unless you know where to start, items such as Cadmium may sneak up on you in unacceptable levels. Economical hazards are, in my opinion, a bit easier to research. When looking at economical hazards, we are basically trying to prevent intentional contamination to gain or profit. In more common terms, this is often referred to as food fraud. Olive oil, fish, and even spices have been known to be the victims of food fraud. There are plenty of informational sites out there to help get you started on writing your hazard analysis for food fraud, however some I have found you do have to pay for.

Another common non-conformance that I see missing in HACCP audits is what I would call inputs and outputs to the HACCP flow chart. Inputs are: Water, compressed air, ice and even steam. Outputs are: Waste, animal feed or by-products. This is not an all-inclusive list, but certainly these examples could bring a new level of hazards to your facility, especially if you did not include them in your hazard analysis. Even worse, if you did include them but decided to write in your hazard analysis that word…dare I even say it… “NONE”: You wrote “none” for biological, chemical, and physical hazards. More than likely you have a pre-requisite program, letter of guarantee, or something that controls these hazards, and you absolutely want to include these in your HACCP plan. Give yourself credit! Auditors and customers alike truly want to see that you have documented and given thought to each of your processing steps. Make sure you take that HACCP flow chart and walk around your facility to ensure you have captured the needed information that will give you the best chance of catching items that can be missed. The plan is only as strong as the time you put into it, which leads me to my next point: Your HACCP or Food Safety Team.

The notorious HACCP team. You have one, the head of the team is the QA manager, and you have team members to cover the multi-disciplinary basis. So, what’s the problem? Well, maybe none, but remember the comment about the golden sticker on your certificate? It’s the same thought process here. Your team must be continually updated and educated to keep up with the ever-changing world of food. That 1999 HACCP certificate is no longer valid in the eyes of some customers. I have seen many customers requiring that HACCP be retrained every five years. For the sites that must follow FSMA rules and regulations, have you completed your Preventative Controls Qualified Individual training? You should have, and who is their backup? It takes much planning and money to make this happen, but it is all a crucial step in maintaining food safety and your HACCP plan.

We all know that our programs and processes are not good for forever and that change is inevitable. There are always avenues for gathering information and accessing it. You must be willing to go out and get the resources that will place an upgrade on your food safety management system, as waiting for it can sometimes cause gaps and non-conformities. The big question is: Did you put in the hours?

Food Safety Consortium

Making Your Supply Chain Smarter, Safer and More Sustainable

By Maria Fontanazza
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Food Safety Consortium

How to build a smarter, safer and more sustainable food supply chain: This was a big topic at the 2018 Food Safety Consortium last month. David McCarthy of IBM Food Trust led a panel of experts from the retail side of the industry in a Q&A session about their biggest challenges in the supply chain, the role of digital and how to achieve a higher level of transparency.

What are the main areas in the supply chain where there’s a major need for improvement?

Sean Leighton, vice president of food safety and quality, Cargill: One of the biggest challenges that I see from a supplier perspective is people’s assumptions around what is the supply chain—our mindsets, our ability to talk with each other on “what do you mean by ‘supply chain’”?

Cindy Jiang and Scott Horsfall at the 2018 Food Safety Consortium
Cindy Jiang and Scott Horsfall (all images credit: amybcreative)

What is food safety’s role in the supply chain?

Cindy Jiang, senior director of worldwide food safety, quality and nutrition, McDonald’s Corp.: The supply chain is a supply network; it’s not linear. The most fundamental thing is to ensure there’s no disruption—that the supply chain can provide goods and food product to your customers. When you’re looking at the supply chain, [there’s a] change between the traditional thinking and the digital demand. How do you provide information in an effective way to your customers?

Howard Popoola, vice president, corporate food technology and regulatory compliance, The Kroger Company: Our supply chain means nothing if we aren’t able to deliver safe foods to those consumers in the last mile. Consumers are thinking about the experience that they’re going to have with this product. They’re not thinking about whether it’s safe or not. They’re thinking about the meal they’re going to make at home with the ingredients that they purchased.

The biggest pain point from the retailer’s perspective, when you look at us as being the last in the chain, is in transparency [and] knowing where the products are coming from. Transparency is very big for us. And it takes more than the retailer to open that door of transparency to the consumer.

What are the challenges you’re seeing in providing transparency?

Scott Horsfall, CEO, California Leafy Greens Marketing Agreement: I think a big challenge right now and in the future is communication.

Leighton: I think the winners….are going to be the ones that try to achieve consumer trust. The future is no place for the three ring binders…it’s digital. Where does the data sit? How can you provide access to them through customers?

Howard Popoola, Sean Leighton, Food Safety Consortium
Howard Popoola and Sean Leighton

How does the digital transformation play into providing transparency?

Popoola: The consumers have already trusted the food industry. There are millions of people walking into retail stores buying product. If the trust isn’t there, they wouldn’t be doing that. We erode that trust when [a consumer] has a terrible experience with that product.

How are you seeing digital transformation across the supply chain?

Jiang: Digital is one of the top three initiatives of McDonalds; how do we connect with consumers? When serving 70 million customers each day, how can we get to the transparency to understand the supply—digital is one of the answers. From the supply chain standpoint, we’re looking at the analytics. We cannot think about only one solution. We have to have different solutions to get the end results.

Popoola: I think the food industry has to see itself as a big ecosystem. If we don’t see ourselves as an ecosystem that strives for the one thing,… digital is always going to be a mirage. We have to look at what is digital and understand the fact that [we have large and small companies]. It’s not going to be one size fits all.

How long will it take the food industry to get to a completely digital operation?

Jiang: Looking at the total industry digitized—the majority of the work can be done within the next five years, [by] looking at leading companies. But in terms of total digitalization of the ood network in the U.S., I think that will take another 10 to 20 years.

Food Safety Consortium
(left to right) Howard Poopola, Sean Leighton, Cindy Jiang, Scott Horsfall and David McCarthy discuss supply chain challenges during the 2018 Food Safety Consortium

Horsfall: I think there’s a challenge with much of the farm community to get to this point. There’s also this issue with how you transmit the information. [Horsfall predicts] 10-15 years for the industry.

Leighton: Even a 100% digitized food industry has limited value if the players in the industry can’t pull together to deliver meaningful insights from it all.

What are the most promising innovations solving transparency?

Jiang: When looking at innovation, not just technology (technology is an enabler)— the most impactful innovation is human innovation: How can we work together? The GFSI platform started 20 years ago, and now it’s so impactful around the globe. [Now we’re] looking at how to harmonize food safety standards.

How can we standardize and harmonize… for ingredient suppliers?
How [can we] use the GS1 platform, numbering system to track on where the ingredient is coming from and how that product is made for us—what’s in my product?

Think about the human collaboration and how to improve where we’re at.

Poopola: I would like to tackle this from a different perspective: When we built technologies (whether off-the-shelf or customized) 20 years ago, we thought [it would be around for] the next 100 years. It’s clear today that the technology you have in place might be obsolete in five years. We have to look at the technology we’re building and acquiring today: Will it be relevant in five years?

Leighton: It’s hard to wrap my head around…deep learning and AI [artificial intelligence]. The insights we can gain from machine learning and predictive analytics. Could AI be human’s last invention?

Horsfall: In produce industry, which hasn’t always been in the front, I think that’s changing. [We’re] trying to bring AI and new technology to bear.

Doug Sutton, Steritech
Retail Food Safety Forum

What Attracts Customers to Your Restaurant, and What Could Keep Them Away Forever?

By Doug Sutton
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Doug Sutton, Steritech

The most recent numbers from Black Box Intelligence reflect what has been an ongoing trend for the last several months—improving same store sales. Sounds like great news, right? It could be, if another key metric wasn’t trending in the wrong direction.

Traffic numbers in restaurants are on a very steady down slope. In the third quarter, traffic was down 1.3%, and in October, traffic slowed down by another 2.2%.

The bottom line: Fewer people are dining out, but they’re spending more money.

For now.

Earlier this year, a survey of 500+ consumers asked them several questions about their preferences and experiences when dining out, as well as how they are making their decisions. The results could help restaurant operators adjust their customer experience to help bring more traffic through the door.

Despite Low Traffic Numbers, Americans Still Dine Out Frequently

Consumers have a lot of choice when purchasing a prepared meal these days: Restaurants or prepared foods from a grocery store? Dine in or take out? Fast food, fast casual, or full-service dining? The list goes on and on.

Sixty percent of the above-mentioned survey takers had dined at a restaurant, whether sit-in or delivery, once a week or more frequently. Another 25% reported doing the same two to three times a month.

But there is stiff competition.

Nearly 70% of the same group has purchased prepared foods (pre-made sushi, fried chicken, sandwiches, etc.) at a grocery or convenience store in the last month, indicating that the convenience of prepared foods is taking root in American life. This is an increase from a similar survey conducted in 2016, when slightly more than 65% of respondents said they had purchased a prepared meal from these sources.

What Are Customers Really Looking for in a Restaurant?

It should come as no surprise, that the driving factor for choosing a restaurant is the quality of the food. Respondents of this survey were provided a list of 10 areas of food safety and operational items to choose from and asked them to choose up to five that matter to them most when choosing a restaurant. Food quality and taste was the frontrunner by far, but restaurant cleanliness was second.

The third item on the list might surprise people. It wasn’t speed of service, or order accuracy, or service quality—while they all do matter to customers, it’s their previous experience with a location or chain that matters most.

When Customers Want Answers about a Restaurant, They Go Online

Social media and online reviews are playing an increasingly important role in how customers share their experiences with restaurants. The news about social media and online review sites is good for restaurants. If you’re doing a good job with your customer experience, your customers are willing to talk about it.

Respondents were extremely likely to use social media to share a restaurant experience on a social media platform such as Facebook, Twitter, or Instagram: 58%, said they would be very or somewhat likely to share a restaurant experience on social media. Even better news? Among those who fell into these two categories, nearly two-thirds say they are more likely to share a positive experience than a negative one.

The same holds true for online restaurant review sites, such as Yelp! And OpenTable. While fewer customers say they are very or somewhat likely to share their experience on an online restaurant review site, 49% of those who use review sites once again say that a positive experience is more likely to garner a review than a negative one. A full 66% of those who would be likely to use an online review site are likely to post a positive experience over a negative one.

Especially in the case of online restaurant review sites, this is important. Why? Because nearly three-quarters of respondents sometimes or often use restaurant review sites to help select where they will dine. Among those respondents, the online review carries significant weight in making their decision. Nearly 25% say online reviews are extremely or very influential in their dining decisions, while another 41% qualified them as moderately influential.

Delivery Problems and Who Customers Blame

Most restaurant operators know that there are big dollars to be had in the delivery space. But, the results of this survey indicate that restaurants have a bit of work to do.

Well over half (58.9%) of those surveyed had ordered food for delivery in the six months before the survey. Of those, nearly 30% experienced a problem with their order: Food being cold, wrong food, took too long to deliver the food, etc.

Here’s the important takeaway for restaurants offering delivery: Whether you manage delivery yourself or use a third-party delivery service, customers that experience problems place the fault squarely on the restaurant. Among those that experienced a delivery problem, 79.55% say the restaurant was to blame. That’s important because with third-party delivery service, the restaurant does lose some control over time it takes to deliver, food security, and more.

Foodborne Illness Outbreaks Have a Long-term Effect on Revenue

A 2018 study from the Johns Hopkins Bloomberg School of Public Health put a price tag on foodborne illness outbreaks for restaurants: Anywhere from $4,000 up to $1.9 million wrapped up in “lost revenue, fines, lawsuits, legal fees, insurance premium increases, inspection costs and staff retraining.”

The survey results discussed in this article show that the effects of a foodborne illness outbreak could linger for much longer than anyone truly realizes.

Nearly 30% of respondents said they would never eat at that location if they knew a foodborne illness outbreak had happened there; 24% said they would stay away for between one to six months, and another 18% said they would stay away for six months to a year.

The responses get more dramatic when chain restaurants have foodborne illness incidents. When asked if they would avoid eating at other locations in the chain if a single location was involved in an outbreak, more than 31% said yes, and a whopping 50% say maybe. The majority of respondents would give the chain a second shot, however. Only 19% say they’d never eat at any location in the chain again; more than half (over 58%) report that they would only stay away for between one month and one year.

If multiple locations of a chain are involved, the percentage of respondents that would avoid eating at other locations in the chain more than doubled to more than 68%. The bulk of those who would stop eating at other locations in the chain (31%) say they’d never eat at the chain again, while another 18.5% would avoid the chain for longer than a year. Another 23% say they’d stay away for six months to one year.

Customer Experience Investments Can Reap Big Rewards

This survey revealed plenty of other details about what customers are looking for—what cleanliness factors drive them crazy, what they think of health department scores (and which groups are really paying attention), what really turns them off when they read it in a review—but the real takeaway is this: Restaurants willing to invest in customer experience and a culture of food safety will reap the rewards from customers.

Lettuce

Latest on E. Coli Outbreak Involving Romaine Lettuce

By Food Safety Tech Staff
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Lettuce

Yesterday FDA issued an update on the E.coli O157:H7 outbreak linked to romaine lettuce grown in California. The agency’s traceback investigation continues, and it is working with the Public Health Agency of Canada (PHAC) and Canadian Food Inspection Agency (CFIA), as there is a similar outbreak in Canada.

FDA stated that the contaminated lettuce likely originates from the Central Coast growing regions of northern and Central California (Counties of Monterey, San Benito, San Luis Obispo, Santa Barbara, Santa Cruz and Ventura).

“Traceback information from four restaurants in three different states so far has implicated 10 different distributors, 12 different growers, and 11 different farms as potential sources of rthe contaminated lettuce. The information indicates that the outbreak cannot be explained by a single farm, grower, harvester, or distributor.”

FDA’s latest update states that 52 illnesses and 19 hospitalizations have been reported across 15 states (the highest cases are in California and New Jersey with 11 illnesses each).

Earlier updates:

(UPDATE) CDC Alert: Do Not Eat Romaine Lettuce, Throw It Out

Mahni Ghorashi, Clear Labs
FST Soapbox

Why the Food Safety Industry Needs the Cloud

By Mahni Ghorashi
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Mahni Ghorashi, Clear Labs

Cloud computing and storage, the breakthrough technology that once dominated headlines, conferences and CIOs’ strategic plans, is now commonplace in most industries. That is not to discount the journey it took to get here, though. This easy acceptance wasn’t always the case, and in fact, some of the world’s most important industries are lagging behind.

Food safety is one such industry that stands to gain the most from adopting cloud technology but continues to rely heavily on manual processes, paperwork, and cumbersome on-premise databases. These methods are seen as fail-safe, proven by history to be effective enough and compatible with the overarching goals of the industry. We’re suffering from the age-old adage: If it isn’t broken, we don’t need to fix it.

While the food safety industry has good reasons for taking a more conservative approach to new technology, I’d argue that the most pressing risk to our industry is the failure to invest in innovation. In our own attempts to avoid risk, we’re actually exposing ourselves to far greater losses both in protecting consumers and new opportunities.

A Path Forward For Food Safety

The food safety industry is changing, and changing rapidly. However, despite advances, the industry still faces major challenges. We’ve seen more than 200 recalls just this year. An average recall costs $10 million dollars in direct costs alone. On average, it takes 57 days to recall food, according to a report by the Office of Inspector General.

At the same time, we’re beginning to generate more data than ever, with technologies like blockchain and next-generation sequencing coming online in a big way. We’re about to experience a data explosion arguably bigger than in any other industry. A single NGS test can give industry officials hundreds of millions of data points per analysis, and routine pathogen tests are happening at high volumes around the clock.

This amount of data cannot be contained in the spreadsheets and on-premise databases of today.

The hesitation to adopt cloud-computing is not unfounded, given the initial fear around outages and security, and a disbelief that the technology could ever be as reliable and secure as their existing systems. And the hesitation is even more understandable when you consider that food and beverage is the third-most hacked industry. The damage from these breaches can be extensive, with reports that 70% of hacked food and beverage companies go out of business within a year of an attack. There is a substantial cost for lax security or prolonged outages.

Clearly, any solution has to be comprehensive, and our justifications for switching systems have to be all the more clear. But we cannot as an industry sit idle.

The food safety industry has an opportunity to learn from those who have gone before us and build a stronger, more robust cloud infrastructure.

We’re starting to see this shift take place – some of the top poultry manufacturers have already made the leap into cloud computing. They and others will prove that the value of making the move far outweighs the risk.

Quality Control and Consistency

Right now, it’s not uncommon for food safety employees to record their observations via paper and pencil. In a best-case scenario, these professionals are forced into spreadsheets with limited interoperability. In either scenario, there are huge amounts of friction when it comes to sharing information and, in fact, data can easily be lost as inboxes fill, software crashes, or papers get buried in the shuffle.

By enabling instantaneous data sharing, the cloud makes collaboration across an organization easily accessible for the first time. This, in turn, boosts productivity and also guarantees a higher degree of consistency in both process and results.

Employees can instantly share results, communicate across departments, and easily control permissions and access to information, allowing others to iterate on or apply their findings in real time.

Speed Across an Organization

The drive to increase efficiency actually underwrites the entire food safety industry. Experts are constantly asking how we can be faster at assessing risk, managing recalls, and generally running a business. These questions are only becoming more important as the threat of foodborne illness continues to rise.

The cloud enables greater speed in tracking food information inside and outside of the lab. Perhaps more than any other tool, cloud technology is going to allow the food safety industry to more quickly and effectively manage recalls.

Technology that allows companies to immediately update information company-wide without the burden or drag of an unwieldy IT infrastructure is valuable. Technology that gives you easily interpretable results, so that you can make quick decisions for the good of public health safety is valuable.

Cloud technology enables both. You could easily process terabytes worth of data and spit out easy, comprehensible results that would have otherwise taken days or weeks to produce.

This ability, which on its own is attractive, is especially important as you get into more complicated pathogen tests. For example, with traditional serotyping, a substantial portion of calls are subjective. The speed of cloud computing can take away some of that guesswork.

Dramatic Cost Savings

Not only does the cloud offer a faster system for storing and accessing information, but it also offers cheaper infrastructure, usually an offshoot of its speed. A survey of more than 1,000 IT professionals found that 88% of cloud users pointed to cost savings and 56% agreed that cloud services had helped them boost profits. Additionally, the absolute cost of the cloud is continuing to drop, improving margins.

With the cost savings enabled by the cloud, the food safety lab no longer has to stay a cost center. Adopting cloud technologies can create more wiggle room in a company’s budget and free up resources for ambitious experiments, new product development, and other activities that contribute to the bottom line of the organization.

Security and Regulatory Advancements

The cloud also allows companies to more easily cooperate with HAACP and FSMA regulations. With all of this organizational data easily available and updated in real time, organizations can ensure they’re keeping pace with regulatory requirements by easily producing traceability records and managing compliance requirements across multiple locations and vendors, for example.

While better, more transparent data management company-wide has always been the draw of cloud, the technology has been crippled by simultaneous concerns about security. Food safety executives feel stuck between wanting to comply with best practices and needing to protect sensitive and valuable information.

Fortunately, food safety has waited long enough. Even as recently as 2015, cloud breaches of major organizations’ databases were still making headlines. However, the technology has come a long way in a short time. Cloud providers are beginning to implement automatic checks of systems to analyze threats and identify their severity.

These advancements speak to the food safety industry’s primary pain points, security and speed. By solving for both, the cloud has reached a maturity worthy of the food safety industry.

The Future: Data Pollination

Finally, the cloud makes it much easier to share data across departments, organizations, and even entire industries.

We’re entering an era of data pollination. What I mean by that is there an opportunity to mesh food safety data (genomic data, label information, etc.) with other forms of data—human microbiome data, for instance, to create “personalized” food, enabling consumers to eat ideal foods based on their genetic makeup. While this trend has already taken off, it could be further improved and better validated by bringing food and genetic data out of their silos.

On the opposite end of the production line, data pollination could also help farmers, who have huge amounts of data at their fingertips, understand how they can play a larger role in food safety. If data can enable farmers to produce bigger yields, data can also certainly help farmers prevent any environmental causes of food safety on the farm itself.

Bringing together the data from the entire lifecycle of food—from farmer to consumer—can only be a good thing, powered by the cloud.

Conclusion

The food industry should not look at the task of updating their infrastructure to the cloud as a burden or an extra cost—it’s an investment and when done right, it can provide far greater returns. We have the advantage of late adoption and learning from the implementation mistakes and successes.

This isn’t just incremental improvement territory—we’re talking about making a quantum leap forward in our industry.

Alert

JBS Recalls More than 12 Million Pounds of Raw Beef, May Be Contaminated with Salmonella

By Food Safety Tech Staff
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Alert

Following an expanded recall issued this week, JBS Tolleson, Inc. has now recalled about 12,093,271 pounds of non-intact raw beef products over concerns that they may be contaminated with Salmonella Newport. The initial recall of nearly 7 million raw beef products occurred just two months ago. The Class I recall announced today involves an additional 5,156,076 pounds of raw beef products that were produced and packed between July 26 and September 7, 2018, according to USDA’s FSIS . The recalled products have the establishment number “EST. 267” inside the USDA mark of inspection.

According to the CDC, there are currently 246 reported Salmonella Newport illnesses across 25 states, with 59 hospitalizations. No deaths have been reported. FSIS and CDC have been working with case patients who have provided receipts or shopper card numbers to conduct traceback investigations. The agencies are urging consumers to check their freezers for any recalled product.

baby

Keeping Baby Food Safe: Sensitive Pesticide Residue Quantitation Beyond Maximum Residue Levels Using GC-MS/MS

By Paul Silcock
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baby

There are more than 1000 different pesticides in use around the world. While these chemicals are designed to target insects, weeds and other pests, residual amounts can remain on food that is subsequently eaten by consumers. The effects of pesticides on the population can be acute or chronic depending on the exposure. Acute over-exposure can cause poisoning and result in long-term effects such as cancer or reproductive issues. Chronic, lower dose exposure to pesticides has been associated with health issues such as respiratory problems, skin conditions, depression, birth defects, cancer and neurological disorders such as Parkinson’s disease.

People who face the greatest risk for adverse health outcomes from pesticide exposure are those in agricultural roles, who are more likely to come into direct contact with these chemicals. However, developing fetuses, infants and children, as well as pregnant and nursing mothers and women of childbearing age are at increased risk of experiencing negative health effects due to the presence of unsafe levels of pesticides in food. Exposure throughout a child’s development¬–including in the womb, infancy, early childhood, and puberty–can be particularly dangerous, affecting hormone regulation and brain development.

To minimize adverse health effects, the United States Environmental Protection Agency (EPA) and the European Union (EU) impose strict regulations on the amount of pesticides that can be applied to a crop, in order to limit the residue exposure downstream. Pesticides are assigned maximum residue levels (MRLs) depending on their toxicity, with the majority typically set at 10 µg/kg. However, due to the greater risk of certain compounds affecting the healthy development of infants and young children, some pesticides are controlled further: For instance, in the EU, specific pesticides are restricted in baby foods with MRLs of between 3–8 µg/kg.

Triple Quadrupole GC-MS/MS: Meeting the Needs of Pesticide Analysis

In order to test foods for pesticide residues at these very low levels, food safety laboratories require sophisticated analyte detection technologies. Gas chromatography-tandem mass spectrometry (GC-MS/MS) is a powerful analytical technique that offers the sensitivity and selectivity required to detect and identify pesticide residues at levels that often go beyond those mandated by regulatory authorities, even in complex sample matrices such as baby food. Indeed, GC-MS/MS can detect multiple residues within samples at levels as low as 0.025 µg/kg, much lower than the MRLs of regulated pesticides.

The sensitivity of the latest triple quadrupole GC-MS/MS systems is enabling levels of detection so low that many food testing laboratories have been able to adopt more efficient and universally-applicable sample preparation procedures based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) methods. Combining these modern GC-MS/MS systems with QuEChERS sample preparation techniques allows food samples to be analyzed directly, significantly reducing workflow complexity. Furthermore, the specificity of triple quadrupole GC-MS/MS can easily compensate for the additional matrix components or residual acetonitrile carried over from sample preparation.

EU SANTE Criteria for Pesticide Residue Quantitation

When it comes to the detection of pesticides in baby foods, workflows must comply with rigorous quality control and method validation standards. The EU SANTE/11813/2017 criteria outline three specific requirements that pesticide residue analysis methods must satisfy to achieve compliance.

Firstly, a minimum of two product ions must be detected for each pesticide with a peak signal-to-noise ratio greater than 3 (or in case noise is absent, a signal must be present in at least five subsequent scans), and the mass resolution for precursor ion isolation must be equal to or better than unit mass resolution. Secondly, the retention time of an analyte within a sample must not differ by more than 0.1 minutes compared with standards in the same sequence. Finally, the relative ion ratio for each analyte must remain within 30% of the average of calibration standards from the same sequence.

Fortunately, modern triple quadrupole GC-MS/MS systems are ensuring food safety testing laboratories comply with these criteria. In terms of peak detection and resolution, the specificities achieved using the latest triple quadrupole instruments meet or exceed the EU SANTE requirements by providing consistent data points regardless of sample preparation approach or matrix type. Precise detection at the ultra-low concentrations required for pesticide residue quantitation is routinely achieved using modern triple quadrupole GC-MS/MS systems, with analyses offering qualitative identification of each analyte among a large group of residues. Furthermore, the latest systems deliver stable ion ratios that are well within the required 30% range at the default 10 µg/kg MRL across multiple injections.

Ultra-low-level Quantification of Pesticides Using Triple Quadrupole GC-MS/MS

In a recent study that put the capabilities of the latest triple quadrupole GC-MS/MS systems to the test, samples of baby food (carrot/potato and apple/pear/banana) spiked with a mixture of more than 200 pesticides at three concentrations (1.0, 2.5 and 10.0 μg/kg) were analyzed using the Thermo Scientific TSQ 9000 triple quadrupole GC-MS/MS system fitted with an Advanced Electron Ionization (AEI) source. Prior to injection into the instrument, the homogenized spiked samples were prepared for analysis using a QuEChERS method that included an acetonitrile extraction step, a clean-up step involving primary secondary amine (PSA) and dispersive solid phase extraction (dSPE), followed by acidification with 5% formic acid in acetonitrile.

The triple quadrupole GC-MS/MS system met all SANTE criteria at the three spiking concentrations in both food matrices. More than 97% of the target pesticide residues in the 1 μg/kg spiked sample had recoveries in the range of 70%–120%, highlighting the broad applicability of the method. The recoveries of the target pesticides from the apple/pear/banana sample spiked at 10 μg/kg are shown in Figure 1.

GC-MS/MS system, pesticide residue analysis
Figure 1. Recovery and precision data for apple/pear/banana extractions (n=6) at a concentration of 10 μg/kg, obtained using TSQ 9000 triple quadrupole GC-MS/MS system fitted with an advanced electron ionization (AEI) source.
GC-MS/MS system
(Figure 1 continued)

Triple Quadrupole GC-MS/MS: Supporting Exceptional Limits of Detection

To determine the limits of detection of the system, baby food samples prepared by the previously-described QuEChERS method were spiked with the same mixture of pesticides at 14 concentrations ranging from 0.025 to 250 μg/kg. Using the triple quadrupole GC-MS/MS system, the SANTE criteria were met for all of the pesticides targeted at the default MRL of 10 μg/kg. Additionally, more than 90% of the target compounds had a limit of identification (LOI) satisfying all SANTE requirements below 0.5 µg/kg, and more than 60% of the target residues met these criteria below 0.1 µg/kg (Figure 2).

Pesticide residue analysis
Figure 2. Number of target residues satisfying the EU SANTE requirements (carrot/potato sample matrix). IDL, instrumental detection limit; LOI, limit of identification.

Instrumental detection limits (IDLs) were also determined for each pesticide residue by performing 10 replicate injections of the lowest matrix-matched standard of carrot/potato that met all SANTE criteria. IDLs were then evaluated using one-tailed student t-tests, taking into account the concentration and absolute peak area %RSD for each compound. The evaluated IDLs ranged from approximately 5 fg (for chlorobenzilate) to 2.0 pg (for bioallethrin), with over 95% of the residues exhibiting an IDL of less than 500 fg on the column (equivalent to 0.5 µg/kg in each sample extract). These results highlight the exceptional performance of the system, offering quantitative analysis of more than 200 pesticides over up to five orders of magnitude.

Conclusion

Enforcing regulations on the amounts and types of pesticides used is essential to limit our exposure to safe levels. The latest GC-MS/MS systems are capable of detecting and identifying pesticide residues at levels far beyond those required under regulatory standards, helping food testing laboratories efficiently ensure the food our children eat is always safe to consume.

Karen Everstine, Decernis
Food Fraud Quick Bites

Recent Notable Incidents

By Karen Everstine, Ph.D.
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Karen Everstine, Decernis

We developed a system that tracks food fraud records using four categories: Incidents, inference records, surveillance records and method records. Food fraud incidents are documented occurrences of fraud that include contextual information about location, perpetrators, timeframe, geographic location and other characteristics. In many ways, incidents are the gold standard of food fraud records. However, there have been unsubstantiated reports of food fraud that were subsequently discredited (such as the “plastic rice” scandal of a few years ago). For this reason, for every incident we capture, we assign a “weight of evidence” classification to provide our assessment of the strength of the evidence. For example, incidents reported directly by regulatory agencies with supporting documentation will generally be assigned a “high” weight of evidence classification.

We also work diligently to avoid “double counting” food fraud incidents, although at times this can be challenging. Incidents may be reported in multiple media outlets and, at times, the reports may not include enough information to determine if it is a new report or related to an issue already reported. We cross-reference the dates and locations of reports, along with information about the ingredients and adulterants, to help ensure that isolated food fraud cases are reported as one incident.

Food fraud, Decernia
Food fraud incidents since 1980. (Source: Decernis Food Fraud Database)

Incidents we have captured in the past two months include $14 million of counterfeit wine discovered in China, which was reportedly based on a tip off. The Carabinieri and ICQRF in Italy discovered wines with added flavorings and other additives. The Guardia di Finanza in Italy also seized adulterated extra virgin olive oil. Counterfeit liquor was discovered in Russia and bootleg liquor containing methanol caused deaths in Malaysia.

Expired (possibly rotting) eggs intended to be powdered and used in food production were discarded by regulatory authorities in India. A customer in China reported that expired carrots were being re-labeled with new dates. Adulterated milk was discovered in Pakistan. In Kenya, reports surfaced of sodium metabisulfite being used on meat to enhance its appearance. Finally, in the United States, two companies were indicted for importing giant squid and selling it domestically as octopus (which usually has a higher retail price) over a period of three years. A review of these reports illustrates how challenging it can be to collect and standardize food fraud information, especially when it is reported in media sources.

Chelle Hartzer, Orkin
Bug Bytes

Not-So-Fantastic Pests and Where to Find Them

By Chelle Hartzer
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Chelle Hartzer, Orkin

Although no two food processing facilities face the exact same pest pressure, there are a few common pests you’re likely to spot. Depending on the type of pests in the surrounding area, different spaces in a building will be more at-risk for an infestation. Pests will feed on and contaminate product, and get into equipment, if undeterred. And considering many pests can be a potential health and safety threat, prevention is important to help protect your bottom line.

Instead of reacting to pest issues, adjust your integrated pest management (IPM) program to take a proactive approach to preventing the following six common pests.

Rodents

Some of the most clever and resilient creatures in the pest world, rodents are a versatile threat to food products. Usually brown or gray, mice and rats can compress their bodies to fit through holes and gaps the size of a dime and a quarter, respectively. Once inside, they reproduce rapidly. A single rat or mouse can produce more than 32 offspring per year. In addition, they can use their sharp teeth to gnaw through packaging and leave urine and feces droppings everywhere they go. All of this makes them an absolute terror once indoors. They’re smart enough to know hiding from humans is their best option, and they’ll even learn from unsuccessful trapping attempts.

Cockroaches

These notorious crawling insects are contaminators, too. Roaches love to get into dirty areas and run all over food contact surfaces, equipment and products, potentially dropping off disease-inducing pathogens on everything they touch. Cockroaches can fit through tiny gaps by flattening their bodies, making them tough (but not impossible!) to keep out. They tend to avoid coming out in the open during daytime hours, as they prefer to hide in the dark. If you spot one running around during the day, then it may be a sign of a larger infestation behind the scenes.

Flies

When flies detect a potential food source, they’re going to head straight for it. Stringent sanitation is the best way to minimize attractants, and keeping doors and other openings closed can help, too. Preventing flies is important, because they’re twice as filthy as cockroaches. In fact, more than 100 pathogens are associated with the housefly alone. These pathogens are transferred when the fly lands on a surface, contaminating the area. If flies are a threat, you should have fly lights placed strategically to reduce the population and monitor where they’re coming from.

Indian Meal Moths

This tiny insect feeds on a wide range of raw and finished goods, and leaves behind frass (insect droppings) that that can lead to major loss of products. If you don’t see the pest itself, which can be reddish-brown and silver-grey in color, you may notice the silk webbing spun by larvae. When someone notices this, immediate action is necessary, as it means the moths are reproducing and may be spreading amongst products in close proximity.

Sawtoothed Grain Beetle

Unable to penetrate most packaging, sawtoothed grain beetles hunt for holes in packaging, which can be one millimeter in diameter, and lay eggs near the opening. Larvae then squeeze through the hole once hatched and begin feeding on product! Although they prefer processed food products like bran, chocolate and oatmeal, they’ll feed on just about anything they can get into. About three millimeters in length, these beetles love moldy, damp conditions, so minimize those attractants as much as possible.

Ants

Everybody has seen or been around ants before, but are you aware that they carry bacteria on their bodies capable of contaminating food? What starts with a few foragers can escalate quickly, as ants leave behind an invisible chemical trail leading other ants straight to a food source. Ants will feed on just about anything depending on the species, so identification is key. Generally only a few millimeters in length and ranging in color from black to red, ants can establish colonies under a building’s foundation, on lawns or in out-of-sight locations indoors.

Watch Out for High-Risk Areas

Understanding the biology of pests helps us to understand what they’re looking for and where they’re most likely to be hiding. Generally speaking, pests are attracted to places able to provide them with the three things they need to survive: Food, water and shelter.

Food doesn’t necessarily mean actual food products of course, as some pests—like cockroaches, flies and ants—will feed on any organic matter they can find. Remember, that includes garbage!

But taking out the trash and ensuring dumpsters are far away from the building aren’t the only ways to reduce pests. Quite the contrary, pests have a myriad of different hiding spots that should be checked by facility staff and a pest management professional regularly.

For starters, don’t overlook the break room. It’s easy to forget to take out the trash, which should be done at least daily depending on waste output. Break rooms also frequently have sinks with drains where food buildup can cause odors that are attractive to pests. Drain flies love this! Wipe down countertops and sweep/vacuum/mop daily to ensure larger food crumbs and debris are taken care of, and make sure your staff knows to clean up any spills immediately. Don’t forget those vending machines—when was the last time they were moved and cleaned underneath and behind?

Equipment can be a hot spot for pests, too. Insects, especially stored product pests, will hide beneath and behind heavy machinery. Pests don’t want to be exposed out in the open, so they’ll hide in small gaps and crevices. And if there is food waste or moisture present, watch out! Those attractants will prove irresistible if allowed to linger for too long, so make sure your cleaning schedule includes sanitation in and around equipment. Never overlook those hard-to-reach areas, or pests will make you pay.

Speaking of hard-to-reach areas, walls are often popular harborage areas for pests. Rodents are perhaps the most dangerous, as they pose a health and safety threat to employees and can contaminate product. Worse still, wiring in walls looks like roots to rodents. They’ll often chew through and create sparks—a potential fire hazard. Rodents are just one of many pests happy to live in your walls, so contact a professional if you notice activity.

Even once food is produced, packaged and stored, pests are still a threat! Stored product pests, like the Indian meal moth and sawtoothed grain beetle, can get into packaged products and live in it. They’ll feed and contaminate the product, then move onto the next, proving costly when large batches have to be thrown out. Thankfully, there are monitoring devices like pheromone traps to help identify where these begin to pop up, but again, you’ll want a professional’s help to ensure these tools are effective.

Don’t wait for pest sightings to occur before taking action. The best approach to pest prevention is a proactive one, and there’s not an insect or animal alive who can outsmart a trained pest management professional. Lingering issues will prove costly with time, as a product infestation or plant shutdown would be a painful hit on your business’s bottom line. Instead, create a plan that accounts for these pests and high-risk areas around your building, and you’ll be able to rest easier knowing you’re prepared for pest invaders.